China cas 109-64-8 factory wholesale 1,3-Dibromopropane at affordable price
- Molecular Formula:C3H6Br2
- Molecular Weight:201.889
- Appearance/Colour:colourless to slightly yellow liquid
- Vapor Pressure:0mmHg at 25°C
- Melting Point:-34 °C(lit.)
- Refractive Index:n20/D 1.524(lit.)
- Boiling Point:167 °C at 760 mmHg
- Flash Point:54.4 °C
- PSA：0.00000
- Density:1.933 g/cm3
- LogP:2.16630
1,3-Dibromopropane(Cas 109-64-8) Usage
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Hazard
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Colorless liquid; sweet odor. Insoluble in water;
soluble in organic solvents. Combustible. |
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Synthesis
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1,3-Dibromopropane can be prepared via the free radical addition between allyl bromide and hydrogen bromide. It can derived from the reaction of propylene glycol with brominated hydrochloric acid. |
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Purification Methods
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1,3-Dibromopropane [109-64-8] M 201.9, f -34.4o, b 63 -63.5o/26mm, 76 -77o/40mm, 9 0o/80mm, 165o/atm, d 4 1.977, n 1.522. Wash the dibromide with dilute aqueous Na2CO3, then water. Dry and fractionally distil it under reduced pressure. [Beilstein 1 IV 216.] |
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General Description
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1,3-Dibromopropane is a dihalogenated propane. It undergoes reduction catalyzed by electrogenerated solution-phase nickel(I) salen and nickel(I) salen confined in a polymer film on the surface of a carbon electrode to afford cyclopropane and propylene, respectively. |
InChI:InChI=1/C3H6Br2/c1-3-5-11-19-15(17)13-9-7-8-10-14(13)16(18)20-12-6-4-2/h7-10H,3-6,11-12H2,1-2H3
109-64-8 Relevant articles
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Freund
, p. 638 (1881)
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Process intensification-assisted conversion of α,ω-alkanediols to dibromides
Mekala, Shekar,Hahn, Roger C.
, p. 630 - 632 (2015)
The increasingly widespread applications...
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Urushibara,Simamura
, p. 323,330 (1939)
-
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Harmon et al.
, p. 2213 (1950)
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ANALYSE STRUCTURALE EN SERIE CYCLOBUTANIQUE. Partie 1. Derives monosubstitues et gem disubstitues du cyclobutane
Karimine, Mohamed,Galsomias, Jacqueline,Lere-Porte, Jean-Pierre,Petrissans, Jean
, p. 321 - 332 (1987)
Methylene bending mode analysis of some ...
Pulse Radiolysis Study on Radical Cations of Alkyl Bromides in Aqueous Solutions
Mohan, H.,Maity, D. K.,Mittal, J. P.
, p. 477 - 484 (1993)
The transient optical absorption bands f...
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Silbert,Tomlinson
, p. 706,709 (1961)
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Method for preparing n-(γ(v)-bromoalkyl)phthalimides
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Page 3-4, (2008/06/13)
The invention concerns a procedure for p...
Synthesis of 1,3-dibromopropane
Fel'dman, D. P.,Stonkus, V. V.,Shimanskaya, M. V.,Avot-s, A. A.
, p. 250 - 253 (2007/10/03)
A method for preparation of 1,3-dibromop...
General Synthesis of Methyl- and Dimethyl-cyclobutanes from Simple 1,3-Diols by Phase Transfer Catalysis
Toeroek, Bela,Molnar, Arpad
, p. 801 - 804 (2007/10/02)
A general method is described for the pr...
109-64-8 Process route
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10035-10-6,12258-64-9
hydrogen bromide
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109-64-8
1,3-dibromo-propane
Conditions
| Conditions |
Yield |
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at 220 ℃;
Ausschluss von Licht;
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at 20 ℃;
Irradiation;
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78-75-1
1,2-Dibromopropane
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594-16-1
2,2-dibromopropane
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109-64-8
1,3-dibromo-propane
Conditions
| Conditions |
Yield |
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beim Erhitzen;
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109-64-8 Upstream products
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503-30-0
trimethylene oxide
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78-75-1
1,2-Dibromopropane
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74-98-6
propane
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142-28-9
1,3-Dichloropropane
109-64-8 Downstream products
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5721-43-7
hexahydro-pyrazolo[1,2-a]pyridazine
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3661-15-2
octahydro-pyridazino[1,2-a]pyridazine
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48152-09-6
1,3-bis-morpholinopropane
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14208-07-2
[1,1'-(propane-1,3-diyl)-bis(pyridinium)] dibromide
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